Thermogravimetric analyzer Discovery TGA

Thermogravimetric analyzer Discovery TGA, TA Instruments coupled with spectrometer Nicolet iS10 FT-IR, Thermo Fisher Scientific for evolved gas analysis.

Specification

General description

  • Very important complementary method for identification of polymeric materials for both, scientist or engineers.
  • TGA determines the amount of the weight change in a material (common weight 10–20 mg) as a function of increasing temperature (up to 1200 °C) or isothermally under defined atmosphere.
  • Sensitive microbalance gives information about the weight change that can be caused by decomposition, oxidation, sublimation, evaporation and electric or magnetic transformation.
  • Connection to the infrared spectrometer allowing analysis of evolved gases during decomposition of the material.

Applications

  • Thermal stability of plastics, composites, copolymers, rubbers, biopolymers, hydrogels, gels.
  • Assessment of filler content in composites (glass fibers, carbon fibers, limestone, soot, montmorillonite etc.).
  • Assessment of quality of supplied polymeric material with respect to amount of additives, colors, fillers.
  • Assessment of humidity in products (biomaterials, food, cosmetics).
  • Investigation of processes such as sublimation, evaporation, chemical reactions (oxidation).
  • Investigation of kinetics of decomposition processes including determination of activation energy.
  • Analysis of evolved gases during thermal degradation utilizing connected infrared spectrometer.

Specifications

  • Analysis of materials from laboratory temperature up to 1200 °C.
  • Solid samples, powders, fibers, hydrogels etc. can be analyzed.
  • Typical sample mass is about 10–20 mg.
  • Assessment under inert (nitrogen) or oxidation (air) atmosphere, atmosphere can be switched during measurement.
  • Linear heating with rates from 0.1 to 500 °C/min, ballistic cooling with the speed 500 °C/min.

Publications

SLÁMEČKA, K.; DROTÁROVÁ, L.; OLIVER URRUTIA, C.; TKACHENKO, S.; REMEŠOVÁ, M.; GEJDOŠ, P.; ČELKO, L.; MONTUFAR JIMENEZ, E., 2025: Low-temperature gas nitriding effects on mechanical and biological properties of open-porous pure titanium produced by robotic micro-extrusion. SURFACE & COATINGS TECHNOLOGY 505, doi: 10.1016/j.surfcoat.2025.132084 (RIGAKU3, LYRA, TGA-DISCOVERY)

Al-Bashaish, S. R., Shaheen, A. A., Assayed, G. A., Ababneh, E., Alsoud, A., Jaber, A. M., Abuamr, A.M., Al Dmour, H., Sobola,D. & Mousa, M. S., 2025: Synergistic effect of low-concentration carbon nanoparticles on enhancing dielectric and conductive properties of polyvinyl alcohol nanocomposites for high-performance electrolytes in solid-state batteries. MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS 323, p. 118772 - , doi: 10.1016/j.mseb.2025.118772 (TGA-DISCOVERY, MIRA-STAN)

Hashemi, A.; Ezati, M.; Paul, R.; Zumberg, I.; Bacovsky, J.; Fohlerova, Z.; Provaznik, V., 2025: Comparative Effects of ZnO, MgO, and CaO Nanoparticles in 3D‐Printed Chitosan–Agarose Scaffolds on Antibacterial and Osteogenic Outcomes. MACROMOLECULAR BIOSCIENCE 25 (12), doi: 10.1002/mabi.202500232 (FTIR, KRATOS-XPS, RIGAKU3, TGA-DISCOVERY)

Details

Guarantor
Petruš, Josef
Site
CEITECNANO
Location
CEITEC - B1.15