Vacuum FTIR Vertex70v + microscope Hyperion 3000 KIT - polarizors
Instrument consists of a combination of Fourier infrared spectrometer with infrared microscope. In the spectrometer, one can perform transmission and reflection experiments on samples dimension of roughly 1 mm2 and more in the full frequency range offered by the spectrometer, 30-14 000 cm-1. The microscope is used for measurements of either small or spatially inhomogeneous samples essentially down to the diffraction limit in the far field, it means roughly 3 at 3000 cm-1. The frequency range is however limited by the microscope detectors to 600-6000 cm-1. The highlight of this microscope is the focal plane array (FPA) detector that allows simultaneous recording of 128x128 matrix of spectra in the frequency range 900-5000 cm-1.
Specification
Methods
Spectrometer Bruker Vertex 80v spectral resolution 0.2 cm-1 spectral range 20-15 000 cm-1 measurement modes: transmission, reflection at 10 and 80 deg sources: Hg lamp, globar, tungsten Infrared microscope Bruker Hyperion 3000 single element MCT detector, spectral range 600-6000 cm-1 array MCT detector 128x128 pixels, spectral range 900-4000 cm-1 fully motorized mapping stage including motorized focusing objectives: reflection and transmission 15x, 36x ATR (attenuated total reflection) grazing incidence transmissionGallery
Publications
PALACIOS CORELLA, M.; ROJAS TIZÓN, J.; PUMERA, M., 2023: Photocatalytic Pt/Ag3VO4 micromotors with inherent sensing capabilities for corroding environments. JOURNAL OF COLLOID AND INTERFACE SCIENCE 631, p. 125 - 10, doi: 10.1016/j.jcis.2022.10.169 (LYRA, KRATOS-XPS, FTIR, RIGAKU3)
POLAT, Ö.; COSKUN, M.; ROUPCOVÁ, P.; SOBOLA, D.; DURMUS, Z.; CAGLAR, M.; ŠIKOLA, T.; TURUT, A., 2022: The Os substitution into Fe sites in LuFeO3 multiferroic and its effects on the electrical and dielectric features. JOURNAL OF ALLOYS AND COMPOUNDS, p. 165035-1 - 14, doi: 10.1016/j.jallcom.2022.165035 (FTIR)
MUNOZ MARTIN, J.; PALACIOS CORELLA, M.; PUMERA, M., 2022: Electrically reading a light-driven molecular switch on 2D-Ti3C2Tx MXene via molecular engineering: towards responsive MXetronics. JOURNAL OF MATERIALS CHEMISTRY A 10 (32), p. 17001 - 8, doi: 10.1039/d2ta03349f (LYRA, KRATOS-XPS, FTIR)
Bricchi, B. R.; Mascaretti, L.; Garattoni, S.; Mazza, M.; Ghidelli, M.; Naldoni, A.; Li Bassi, A., 2022: Nanoporous Titanium (Oxy)nitride Films as Broadband Solar Absorbers. ACS APPLIED MATERIALS AND INTERFACES 14 (16), p. 18453 - 18463, doi: 10.1021/acsami.2c01185 (FTIR)
Kozak, A.; Hofbauerová, M.; Halahovets, Y.; Pribusová-Slušná, L.; Precner, M.; Mičušík, M.; Orovčík, L'.; Hulman, M.; Stepura, A.; Omastová, M.; Šiffalovič, P.; Ťapajna, M., 2022: Nanofriction Properties of Mono- and Double-Layer Ti3C2TX MXenes. ACS APPL MATER INTER 14 (32), p. 36815 - 10, doi: 10.1021/acsami.2c08963 (FTIR)
Jancik-Prochazkova, A.; Mayorga-Martinez, C. C.; Vyskočil, J.; Pumera, M., 2022: Swarming Magnetically Navigated Indigo-Based Hydrophobic Microrobots for Oil Removal. ACS APPLIED MATERIALS & INTERFACES 14 (40), p. 45545 - 45552, doi: 10.1021/acsami.2c09527 (LEICACOAT-NANO, MIRA-STAN, FTIR)
MUNOZ MARTIN, J.; PALACIOS CORELLA, M.; GOMEZ PEREZ, I.; ZAJÍČKOVÁ, L.; PUMERA, M., 2022: Synthetic Nanoarchitectonics of Functional Organic-Inorganic 2D Germanane Heterostructures via Click Chemistry. ADVANCED MATERIALS 45 (34), doi: 10.1002/adma.202206382 (LYRA, ICON-SPM, KRATOS-XPS, RIGAKU3, FTIR, WITEC-RAMAN)
PALACIOS CORELLA, M.; MUNOZ MARTIN, J.; PUMERA, M., 2022: Molecularly "clicking" active moieties to germanium-based inorganic 2D materials. NANOSCALE 14 (48), p. 18167 - 8, doi: 10.1039/d2nr04955d (LYRA, KRATOS-XPS, FTIR, WITEC-RAMAN, RIGAKU3)
MICHLÍČEK, M.; BLAHOVÁ, L.; DVOŘÁKOVÁ, E.; NEČAS, D.; ZAJÍČKOVÁ, L., 2021: Deposition penetration depth and sticking probability in plasma polymerization of cyclopropylamine. APPLIED SURFACE SCIENCE 540, p. 1 - 10, doi: 10.1016/j.apsusc.2020.147979 (WOOLLAM-VIS, LYRA, FTIR, KRATOS-XPS)
Černohorský, P.; Pisarenko, T.; Papež, N.; Sobola, D.; Ţălu, Ş.; Částková, K.; Kaštyl, J.; Macků, R.; Škarvada, P.; Sedlák, P., 2021: Structure Tuning and Electrical Properties of Mixed PVDF and Nylon Nanofibers. MATERIALS 14 (20), doi: 10.3390/ma14206096 (FTIR, WITEC-RAMAN, KRATOS-XPS, LYRA, HELIOS, LEICACOAT-STAN)
KELAROVÁ, Š.; STUPAVSKÁ, M.; HOMOLA, V.; PŘIBYL, R.; ZÁBRANSKÝ, L.; CHARVÁTOVÁ CAMPBELL, A.; HAVLÍČEK, M.; BURŠÍKOVÁ, V.; VÁCLAVÍK, R., 2021: Stability of trimethylsilyl acetate-based plasma polymers towards atmospheric and water environments. POLYMER DEGRADATION AND STABILITY 190, p. 109628-1 - 14, doi: 10.1016/j.polymdegradstab.2021.109628 (FTIR, ICON-SPM)
ORUDZHEV, F.; RAMAZANOV, S.; SOBOLA, D.; KASPAR, P.; TRČKA, T.; ČÁSTKOVÁ, K.; KAŠTYL, J.; ZVEREVA, I.; WANG, C.; SELIMOV, D.; GULAKHMEDOV, R.; ABDURAKHMANOV, M.; SHUAIBOV, A.; KADIEV, M., 2021: Ultrasound and water flow driven piezophototronic effect in self-polarized flexible alpha-Fe2O3 containing PVDF nanofibers film for enhanced catalytic oxidation. NANO ENERGY 90, p. 1 - 13, doi: 10.1016/j.nanoen.2021.106586 (FTIR, KRATOS-XPS, HELIOS, JAZ3-CHANNEL, LEICACOAT-STAN, WITEC-RAMAN)
SOBOLA, D.; KASPAR, P.; ČÁSTKOVÁ, K.; DALLAEV, R.; PAPEŽ, N.; SEDLÁK, P.; TRČKA, T.; ORUDZHEV, F.; KAŠTYL, J.; WEISER, A.; KNÁPEK, A.; HOLCMAN, V., 2021: PVDF Fibers Modification by Nitrate Salts Doping. POLYMERS 13 (15), p. 1 - 15, doi: 10.3390/polym13152439 (KRATOS-XPS, FTIR, RIGAKU3, LYRA, WITEC-RAMAN, JAZ3-CHANNEL)
Shabanov, N. S.; Rabadanov, K. Sh.; Gafurov, M. M.; Isaev, A. B.; Sobola, D. S.; Suleimanov, S. I.; Amirov, A. M.; Asvarov, A. Sh., 2021: Lignin-Based Gel Polymer Electrolyte for Cationic Conductivity. POLYMERS 13 (14), doi: 10.3390/polym13142306 (FTIR)
Mrkyvkova, N.; Cernescu, A.; Futera, Z.; Nebojsa, A.; Dubroka, A.; Sojkova, M.; Hulman, M.; Majkova, E.; Jergel, M.; Siffalovic, P.; Schreiber, F., 2021: Nanoimaging of Orientational Defects in Semiconducting Organic Films. THE JOURNAL OF PHYSICAL CHEMISTRY C 125 (17), p. 9229 - 9235, doi: 10.1021/acs.jpcc.1c00059 (FTIR)
KASPAR, P.; SOBOLA, D.; ČÁSTKOVÁ, K.; DALLAEV, R.; ŠŤASTNÁ, E.; SEDLÁK, P.; KNÁPEK, A.; TRČKA, T.; HOLCMAN, V., 2021: Case Study of Polyvinylidene Fluoride Doping by Carbon Nanotubes. MATERIALS 14 (6), p. 1428-1 - 12, doi: 10.3390/ma14061428 (RIGAKU3, VERIOS, WITEC-RAMAN, KRATOS-XPS, FTIR)
OLIVER, C.; IBANEZ, R.; FLORES-MERINO, M.; VOJTOVÁ, L.; ŠALPLACHTA, J.; ČELKO, L.; KAISER, J.; MONTUFAR JIMENEZ, E., 2021: Lyophilized Polyvinylpyrrolidone Hydrogel for Culture of Human Oral Mucosa Stem Cells. MATERIALS 14 (1), p. 1 - 14, doi: 10.3390/ma14010227 (FTIR, WITEC-RAMAN, LYRA)
KASPAR, P.; SOBOLA, D.; ČÁSTKOVÁ, K.; KNÁPEK, A.; BURDA, D.; ORUDZHEV, F.; DALLAEV, R.; TOFEL, P.; TRČKA, T.; GRMELA, L.; HADAŠ, Z., 2020: Characterization of Polyvinylidene Fluoride (PVDF) Electrospun Fibers Doped by Carbon Flakes. POLYMERS 12 (12), p. 2766-1 - 15, doi: 10.3390/polym12122766 (VERIOS, KRATOS-XPS, WITEC-RAMAN, RIGAKU3, FTIR)
GHOSH, K.; NG, S.; IFFELSBERGER, C.; PUMERA, M., 2020: Inherent impurities in graphene/polylactic acid filament strongly influence on the capacitive performance of 3D-printed electrode. CHEMISTRY-A EUROPEAN JOURNAL 26 (67), p. 15746 - 8, doi: 10.1002/chem.202004250 (VERIOS, KRATOS-XPS, WITEC-RAMAN, RIGAKU3, FTIR)
Papez, N; Gajdos, A; Sobola, D; Dallaev, R; Macku, R; Skarvada, P; Grmela, L, 2020: Effect of gamma radiation on properties and performance of GaAs based solar cells. APPLIED SURFACE SCIENCE 527, p. 146766-1 - 146766-11, doi: 10.1016/j.apsusc.2020.146766 (LYRA, WOOLLAM-VIS, SIMS, FTIR, WITEC-RAMAN)
Mohelský, I., 2020: Infrared magneto–spectroscopy of Bi2Te3 topological insulator. MASTER'S THESIS, p. 1 - 49 (FTIR, WOOLLAM-MIR, MAGNETRON, CRYOGENIC, KRATOS-XPS)
Mohelský, I.; Dubroka, A.; Wyzula, J.; Slobodeniuk, A.; Martinez, G.; Krupko, Y.; Piot, B. A.; Caha, O.; Humlíček, J.; Bauer, G.; Springholz, G.; Orlita, M., 2020: Landau level spectroscopy of Bi2Te3. PHYSICAL REVIEW B 102 (8), p. 085201-1 - 085201-11, doi: 10.1103/PhysRevB.102.085201 (WOOLLAM-MIR, FTIR)
KŘÁPEK, V.; KONEČNÁ, A.; HORÁK, M.; LIGMAJER, F.; STÖGER-POLLACH, M.; HRTOŇ, M.; BABOCKÝ, J.; ŠIKOLA, T., 2020: Independent engineering of individual plasmon modes in plasmonic dimers with conductive and capacitive coupling. NANOPHOTONICS 9 (3), p. 623 - 10, doi: 10.1515/nanoph-2019-0326 (HELIOS, MIRA-EBL, TITAN, LEICACOAT-STAN, FTIR, EVAPORATOR)
LIGMAJER, F.; HORÁK, M.; ŠIKOLA, T.; FOJTA, M.; DAŇHEL, A., 2019: Silver Amalgam Nanoparticles and Microparticles: A Novel Plasmonic Platform for Spectroelectrochemistry. JOURNAL OF PHYSICAL CHEMISTRY C (PRINT) 123 (27), p. 16957 - 8, doi: 10.1021/acs.jpcc.9b04124 (VERIOS, TITAN, FTIR, WOOLLAM-MIR)
HORÁK, M.; KŘÁPEK, V.; HRTOŇ, M.; KONEČNÁ, A.; LIGMAJER, F.; STÖGER-POLLACH, M.; ŠAMOŘIL, T.; PATÁK, A.; ÉDES, Z.; METELKA, O.; BABOCKÝ, J.; ŠIKOLA, T., 2019: Limits of Babinet’s principle for solid and hollow plasmonic antennas. SCIENTIFIC REPORTS 9, p. 1 - 11, doi: 10.1038/s41598-019-40500-1 (FTIR, HELIOS, LYRA, MAGNETRON, TITAN)
Michlíček, M.; Manakhov, A.; Dvořáková, E.; Zajíčková, L., 2019: Homogeneity and penetration depth of atmospheric pressure plasma polymerization onto electrospun nanofibrous mats. APPLIED SURFACE SCIENCE 471, p. 835 - 841, doi: 10.1016/j.apsusc.2018.11.148 (LYRA, MAGNETRON, FTIR, KRATOS-XPS)
PERMYAKOVA, E.; POLČÁK, J.; SLUKIN, P.; IGNATOV, S.; GLOUSHANKOVA, N.; ZAJÍČKOVÁ, L.; SHTANSKY, D.; MANAKHOV, A., 2018: Antibacterial biocompatible PCL nanofibers modified by COOH-anhydride plasma polymers and gentamicin immobilization. MATERIALS AND DESIGN 153, p. 60 - 11, doi: 10.1016/j.matdes.2018.05.002 (FTIR, KRATOS-XPS)
Rovenská, K., 2018: Metallic nanostructures with three-dimensional topography for plasmonics. BACHELOR THESIS, p. 1 - 45 (MIRA-EBL, EVAPORATOR, FTIR)
BŘÍNEK, L.; KVAPIL, M.; ŠAMOŘIL, T.; HRTOŇ, M.; KALOUSEK, R.; KŘÁPEK, V.; SPOUSTA, J.; DUB, P.; VARGA, P.; ŠIKOLA, T., 2018: Plasmon Resonances of Mid-IR Antennas on Absorbing Substrate: Optimization of Localized Plasmon-Enhanced Absorption upon Strong Coupling Effect. ACS PHOTONICS 5 (11), p. 4378 - 8, doi: 10.1021/acsphotonics.8b00806 (LYRA, FTIR)
Ligmajer, F., 2018: Advanced plasmonic materials for metasurfaces and photochemistry. PH.D. THESIS, p. 1 - 142 (VERIOS, ICON-SPM, RIGAKU9, FTIR, WOOLLAM-VIS, TITAN)
Dvořák, P., 2018: Nanophotonics. PH.D. THESIS, p. 1 - 134 (LYRA, EVAPORATOR, FTIR, WOOLLAM-VIS)
LIGMAJER, F.; KEJÍK, L.; TIWARI, U.; QIU, M.; NAG, J.; KONEČNÝ, M.; ŠIKOLA, T.; JIN, W.; HAGLUND, R.; APPAVOO, K.; LEI, D., 2018: Epitaxial VO2 nanostructures: A route to large-scale, switchable dielectric metasurfaces. ACS PHOTONICS 5 (7), p. 2561 - 7, doi: 10.1021/acsphotonics.7b01384 (RIGAKU9, ICON-SPM, VERIOS, FTIR)
MANAKHOV, A.; KIRYUKHANTSEV-KORNEEV, P.; MICHLÍČEK, M.; PERMYAKOVA, E.; DVOŘÁKOVÁ, E.; POLČÁK, J.; POPOV, Z.; VISOTIN, M.; SHTANSKY, D., 2018: Grafting of carboxyl groups using CO2/C2H4/Ar pulsed plasma: Theoretical modeling and XPS derivatization. APPLIED SURFACE SCIENCE 435, p. 1220 - 8, doi: 10.1016/j.apsusc.2017.11.174 (FTIR, KRATOS-XPS)